HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → 3beta-Carboethoxyandrost-5-ene-7,17-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | 7-Keto-dehydroepiandrosterone | HCID 193313 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 3beta-Carboethoxyandrost-5-ene-7,17-dione | HCID 10237086 | 90% |
Reaction Steps
Prepared from (2) and ethylchloroformate in pyridine at 0-5° C. Yield 90%, m.p. 187-8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07947846B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-50e1245c27cc44c5baaf2447c135f5a9 |
| Source note | uspto-grants-2011_05 |