HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 1-aminocyclopentane-1-carboxylate--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Cycloleucine | HCID 2901 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Ethyl 1-aminocyclopentane-1-carboxylate--hydrogen chloride (1/1) | HCID 3028134 | 93% |
Reaction Steps
This was synthesised according to Standard Procedure 1, using 1-amino-1-cyclopentanecarboxylic acid (5.0 g, 38.6 mmol) with thionyl chloride (5.72 mL, 58 mmol) and anhydrous ethanol (29 mL). The product was isolated as a white solid (6.98 g, yield 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951787B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-abe7be6ca4e0492c86db4da8cdfbc3f6 |
| Source note | uspto-grants-2011_05 |