HRID55240

反应详情

EQUATION

反应方程式

HRID 55240 的结构方程式

PROCEDURE

实验过程

As described for Example 8, 0.50 g of 10,11-dihydro-10-(4-aminobenzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine is reacted with 0.483 g of 2,3,5-trichlorobenzoyl chloride to give a glass which is crystallized from ethyl acetate to give 0.686 g of crystals, m.p. 231°-234° C.

WORKUP

后处理

  1. customto give a glass which
  2. customis crystallized from ethyl acetate