m-Anisoyl chloride → HCID 58024296, compound

Participants

Reaction Steps

Method H was used with 7-(3-aminophenoxy)-1H-imidazo[4,5-b]pyridin-2(3H)-one and 3-methoxy-benzoyl chloride to afford the title compound as a brown solid (21 mg, 40%). 1H-NMR (δ, ppm, DMSO-d6): 3.83 (s, 3H, OMe), 6.49 (d, 1H, HPy,5, J=5.8 Hz), 6.90 (d, 1H, Harom, J=7.48 Hz), 7.16 (d, 1H, Harom, J=6.52 Hz), 7.39-7.49 (m, 3H, Harom), 7.52 (d, 1H, Harom, J=7.61 Hz), 7.62-7.68 (m, 2H, Harom), 7.81 (d, 1H, HPy,6, J=5.44 Hz), 10.31 (s, 1H, NHamide), 11.19 (s, 1H, NHPy3), 11.39 (s, 1H, NHPy2).

Provenance & Evidence