HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → 3,6-Dimethyl-4-nitro-pyridine-2-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | Pyridine, 2,5-dimethyl-4-nitro-, 1-oxide | HCID 146707 | — |
| Product | 3,6-Dimethyl-4-nitro-pyridine-2-carbonitrile | HCID 67163003 | — |
Reaction Steps
The title compound, was prepared by treatment of 2,5-Dimethyl-4-nitropyridine-N-oxide (CAS: [21816-42-2], J. Heterocyclic Chem. 34(3), 727(1997)) with Dimethylsulfate and Potassium cyanide in accordance with the general method of example 1, step 1 to yield the title compound as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951824B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-14385ba4eaa24ef9a66647ff5ea71bae |
| Source note | uspto-grants-2011_05 |