HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-5-methylpyridine → HCID 24820893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-5-methylpyridine | HCID 817713 | — |
| Reactant | 2-Pyridinecarboxamide, 6-methyl-N-(4-methyl-2-thiazolyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-YL)- | HCID 49760412 | — |
| Product | HCID 24820893 | HCID 24820893 | — |
Reaction Steps
The title compound, was prepared from 6-Methyl-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-pyridine-2-carboxylic acid (4-methyl-thiazol-2-yl)-amide in accordance with the general method of example 131, step 2 using 5-Bromo-3-picolin instead of 3-Trifluoromethyl-5-bromopyridine to yield the final compound as a white solid, MS (ISP): m/e=325.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951824B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-bfe0ca1f176a44f89b737dce5352bb4e |
| Source note | uspto-grants-2011_05 |