HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-methylpyridine → 2'-Chloro-6-methyl-[4,4']bipyridinyl-2-carboxylic acid (5-methyl-pyridin-2-yl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-methylpyridine | HCID 15348 | — |
| Reactant | 2'-Chloro-6-methyl-[4,4']bipyridinyl-2-carboxylic acid ethyl ester | HCID 86614590 | — |
| Product | 2'-Chloro-6-methyl-[4,4']bipyridinyl-2-carboxylic acid (5-methyl-pyridin-2-yl)-amide | HCID 86614593 | — |
Reaction Steps
The title compound, was prepared from 2′-Chloro-6-methyl-[4,4′]bipyridinyl-2-carboxylic acid ethyl ester in accordance with the general method of example 26, step 6 using 2-amino-5methylpyridine instead of 3-chloroaniline to yield the final compound as a white crystalline, MS (ISP): m/e=339.2, 341.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951824B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-2dcb496017064c1bb901cbe7b65c229d |
| Source note | uspto-grants-2011_05 |