Chlorosulfamic acid → HCID 10066766, compound

HRID 552715Notes

Reaction equation

HRID 552715 reaction equation
[C:1]([O:4][C@@H:5]1[C@H:9]([O:10][C:11](=[O:13])[CH3:12])[C@@H:8]([CH2:14][OH:15])[O:7][C@H:6]1[O:16][C:17](=[O:19])[CH3:18])(=[O:3])[CH3:2].Cl[S:21]([NH2:24])(=[O:23])=[O:22]>>[C:1]([O:4][C@@H:5]1[C@H:9]([O:10][C:11](=[O:13])[CH3:12])[C@@H:8]([CH2:14][O:15][S:21](=[O:23])(=[O:22])[NH2:24])[O:7][C@H:6]1[O:16][C:17](=[O:19])[CH3:18])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 11022150HCID 11022150, compound

Product 1

HCID 10066766HCID 10066766, compound

Procedure

The title compound was prepared from (2S,3R,4R,5R)-2,4-diacetoxy-5-hydroxymethyl-tetrahydro-furan-3-yl acetate by reaction with chlorosulfonamide following a procedure analogous to that described in Example 43, step f.

Sources & evidence

ORD record
ord-96c68273291c4cd6958b3fded5d61534
Source dataset
uspto-grants-2011_05
Patent number
US07951810B2

Reaction notes

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