HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl but-2-enoate → 3-(4-Nitro-imidazol-1-yl)-butyric acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl but-2-enoate | HCID 12181 | — |
| Reactant | HCID 178526856 | HCID 178526856 | — |
| Product | 3-(4-Nitro-imidazol-1-yl)-butyric acid methyl ester | HCID 43536402 | — |
Reaction Steps
4-nitroimidazole was reacted with methyl-3-methylacrylate to provide the title compound: 1H NMR (400 MHz, CDCl3) 1.62 (d, 3H, J=7.0 Hz), 2.81 (d, 2H, J=7.0 Hz), 3.66 (s, 3H), 4.78 (m, 1H), 7.53 (d, 1H, J=1.6 Hz), 7.82 (d, 1H, J=1.6 Hz); MS m/z 214.1 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951958B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-843d3104a430435b81059a0383434546 |
| Source note | uspto-grants-2011_05 |