Ethanamine, 2,2,2-trifluoro- → [2-Methyl-2-(4-nitro-imidazol-1-yl)-propyl]-(2,2,2-trifluoro-ethyl)-amine

Participants

Role	Name	HCID	Charge
Reactant	Ethanamine, 2,2,2-trifluoro-	HCID 9773	—
Reactant	2-Methyl-2-(4-nitro-imidazol-1-yl)-propionaldehyde	HCID 86600809	—
Product	[2-Methyl-2-(4-nitro-imidazol-1-yl)-propyl]-(2,2,2-trifluoro-ethyl)-amine	HCID 67163871	—

Reaction Steps

2-Methyl-2-(4-nitro-imidazol-1-yl)-propionaldehyde was reacted with 2,2,2-trifluoro-ethyl amine to provide the title compound: H1 NMR (400 MHz, CDCl3) 1.59 (s, 6H), 2.98 (s, 2H), 3.10 (m, 2H), 7.56 (s, 1H), 7.90 (s, 1H) MS m/z 267.3 (M+1).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07951958B2
Source dataset	uspto-grants-2011_05
ORD ID	ord-1a31f8eceef44bf18d2bcc0b04e650c7
Source note	uspto-grants-2011_05