HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-2-Hydroxy-3-methylbutanoic acid → HCID 11646642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-2-Hydroxy-3-methylbutanoic acid | HCID 853180 | — |
| Reactant | 2-[4-(2-Amino-pentanoylamino)-imidazol-1-yl]-2-methyl-propionic acid methyl ester | HCID 67165426 | — |
| Product | HCID 11646642 | HCID 11646642 | — |
Reaction Steps
2-[4-(2-Amino-pentanoylamino)-imidazol-1-yl]-2-methyl-propionic acid methyl ester was coupled with (S)-2-hydroxy-3-methyl-butyric acid to provide the title compound: C13 NMR (100 MHz, CDCl3) 13.8, 15.9, 19.1, 19.4, 26.1, 26.2, 32.1, 35.5, 52.6, 53.3, 61.2, 76.4, 106.1, 131.9, 137.5, 169.6, 172.6, 173.9; MS 383.2 m/z (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951958B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-21d14df268ee414b9179d76408b4ad57 |
| Source note | uspto-grants-2011_05 |