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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 553136Generated: October 29, 2026

Methylamine → HCID 11676146, compound

https://huagongshe.com/reaction/553136

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
ReactantHCID 86600811HCID 86600811—
ProductHCID 11676146HCID 11676146—

Reaction Steps

2-[2-(3,5-Difluoro-phenyl)-acetylamino]-pentanoic acid [1-(1,1-dimethyl-2-oxo-ethyl)-1H-imidazol-4-yl]-amide was reacted with methylamine to afford the title compound: C13 NMR (100 MHz, CDCl3) 13.9, 19.0, 26.5, 26.6, 36.0, 37.2, 43.1, 46.0, 53.2, 58.8, 62.6, 102.6, 102.8, 103.1, 105.1, 112.3, 112.6, 131.6, 137.8, 138.8, 162.0, 164.5, 169.2, 169.3; MS m/z 422.2 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07951958B2
Source datasetuspto-grants-2011_05
ORD IDord-5c6ace59e8114650b9031e245422a240
Source noteuspto-grants-2011_05