HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,7-Dimethyl-2-tetralone → HCID 11590818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,7-Dimethyl-2-tetralone | HCID 10397276 | — |
| Reactant | 2-Amino-pentanoic acid [1-(1,1-dimethyl-2-pyrrolidin-1-yl-ethyl)-1H-imidazol-4-yl]-amide | HCID 67164226 | — |
| Product | HCID 11590818 | HCID 11590818 | — |
Reaction Steps
2-Amino-pentanoic acid [1-(1,1-dimethyl-2-pyrrolidin-1-yl-ethyl)-1H-imidazol-4-yl]-amide was reacted with 5,7-dimethyl-3,4-dihydro-1H-naphthalen-2-one to provide the title compound: C13 NMR (100 MHz, CDCl3) 14.2, 19.5, 19.6, 21.0, 24.3, 25.3, 25.6, 26.6, 29.7, 30.7, 36.6, 37.1, 38.0, 53.0, 53.3, 56.0, 59.1, 60.4, 60.8, 67.3, 104.7, 127.9, 28.0, 128.6, 128.7, 131.1, 131.3, 131.6, 134.6, 135.1, 135.2, 136.4, 137.3, 172.5, 172.6; MS m/z 466.5 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07951958B2 |
| Source dataset | uspto-grants-2011_05 |
| ORD ID | ord-c4b9bbe7bdde4a3a863902ee29cd881e |
| Source note | uspto-grants-2011_05 |