Phenylboronic Acid → HCID 57671473, compound

Participants

Reaction Steps

The title compound was prepared similarly to the procedures described for Example 2 from tert-butyl 2-(7-bromo-4-hydroxy-1-methyl-2-oxo-1,2-dihydro-1,5-naphthyridine-3-carboxamido)acetate (Example 1 (f)) and phenylboronic acid. MS (ESI, pos. ion) m/z: 354 (M+1). 1H NMR (400 MHz, CD3OD) δ ppm: 8.86 (s, 1 H), 8.20 (s, 1 H), 7.84 (d, J=7.4 Hz, 2 H), 7.44-7.63 (m, 3 H), 4.16 (s, 2 H), 3.78 (s, 3 H).

Provenance & Evidence