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HRID55363

反应详情

EQUATION

反应方程式

HRID 55363 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：Cc1c(C(=O)NN2CCCCC2)nn(-c2ccc(Cl)cc2Cl)c1-c1ccc(Cl)cc1
HCID104850

Rimonabant

C22H21Cl3N4O

PRODUCTS

生成物

1
结构：Cc1c(C(=O)NN2CCCCC2)nn(-c2ccc(Cl)cc2Cl)c1-c1ccc(Cl)cc1.O=S(=O)(O)O
HCID25026422

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

0.018 ml of concentrated sulfuric acid are added to a solution of 0.30 g of the compound obtained in example 195 in 3 ml of acetone. The white crystals formed are filtered off, washed with acetone and then ether, and dried under vacuum to give 0.31 g of the expected salt. m.p.=240° C.

WORKUP

后处理

  1. customThe white crystals formed
  2. filtrationare filtered off
  3. washwashed with acetone
  4. dry with materialether, and dried under vacuum