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HRID553667

反应详情

EQUATION

反应方程式

HRID 553667 的结构方程式

REACTANTS

反应物

3
结构：CCO
HCID702

Ethanol

C2H6O

结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：O=C(O)Cc1ccc(F)c(Br)c1
HCID3416339

3-Bromo-4-fluorophenylacetic Acid

C8H6BrFO2

PRODUCTS

生成物

1
结构：CCOC(=O)Cc1ccc(F)c(Br)c1
HCID58539475

未命名化合物

PROCEDURE

实验过程

3-Bromo-4-fluorophenylacetic acid (2.35 g, 9.0 mmol) was treated with concentrated sulfuric acid (2 mL) in ethanol (100 mL) at reflux for 2 hours. Purification by silica gel chromatography provided the title compound.

WORKUP

后处理

  1. temperatureat reflux for 2 hours
  2. customPurification by silica gel chromatography