Tributylstannane → 2-Propen-1-ol, 3-(tributylstannyl)-, (Z)-

Participants

Reaction Conditions

Reaction Steps

To neat propargyl alcohol (1 ml) were added tributyl stannane (5.8 ml) followed by 1,1′-azobis(cyclohexanecarbonitrile) (213 mg). The mixture was heated for 2 h at 80° C., cooled to RT, and directly purified by column chromatography (EA/Hept 4/96 to 5/95) to afford 2.98 g of the desired product.

Provenance & Evidence