HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Caprolactam
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Caprolactam | HCID 7768 | — |
| Reactant | beta-Methylstyrene | HCID 12500 | — |
| Product | Caprolactam | HCID 7768 | — |
| Product | HCID 86630203 | HCID 86630203 | — |
Reaction Steps
A mixture of styrene and methyl styrene (40 weight %, including 30 weight % styrene and 10 weight % methyl styrene) and molten caprolactam were mixed and stirred at a constant temperature of 100° C., and 0.05 weight % AIBN was added to initiate the free radical polymerization, giving a solution of styrene-methyl styrene co-polymer/caprolactam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048967B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-8d9ea9a650604d3c979681beb4713e4b |
| Source note | uspto-grants-2011_11 |