HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzenesulfonyl chloride → HCID 66924750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzenesulfonyl chloride | HCID 9588 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 2-methyl-5-phenyl-1H-pyrrole-3-carboxylate | HCID 12258777 | — |
| Product | HCID 66924750 | HCID 66924750 | 32% |
Reaction Steps
Using ethyl 2-methyl-5-phenyl-1H-pyrrole-3-carboxylate (500 mg), sodium hydride (60% in oil, 175 mg) and 4-fluorobenzenesulfonyl chloride (848 mg), a procedure as in Reference Example 4 was performed to give the title compound as a brown oil (yield 270 mg, 32%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-b1b1e29c993b44a49964ff0aeab514a9 |
| Source note | uspto-grants-2011_11 |