HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → Ethyl 5-bromo-4-methyl-1H-pyrrole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Ethyl 4-methyl-1h-pyrrole-3-carboxylate | HCID 235044 | — |
| Product | Ethyl 5-bromo-4-methyl-1H-pyrrole-3-carboxylate | HCID 66925114 | 76.7% |
Reaction Steps
Using ethyl 4-methyl-1H-pyrrole-3-carboxylate (4.50 g) and N-bromosuccinimide (5.2 g), a procedure as in Reference Example 40 was performed to give the title compound as a pale-yellow solid (yield 5.20 g, 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-83d9a479dba5497c8dbb21ed2102d192 |
| Source note | uspto-grants-2011_11 |