HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tosylmethyl isocyanide → HCID 66924650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tosylmethyl isocyanide | HCID 161915 | — |
| Reactant | Methyl (2E)-4-methyl-2-pentenoate | HCID 5362843 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Product | HCID 66924650 | HCID 66924650 | 54% |
Reaction Steps
Using p-toluenesulfonylmethyl isocyanide (7.6 g), methyl (2E)-4-methylpent-2-enoate (5.0 g) and potassium tert-butoxide (5.25 g), a procedure as in Reference Example 39 was performed to give the title compound as a pale-yellow oil (yield 3.5 g, 54%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-28f0ea42c8d94945afa447292ea7a082 |
| Source note | uspto-grants-2011_11 |