HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → Methyl 5-bromo-4-propyl-1H-pyrrole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Methyl 4-propyl-1H-pyrrole-3-carboxylate | HCID 53632572 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | Methyl 5-bromo-4-propyl-1H-pyrrole-3-carboxylate | HCID 66924577 | 72% |
Reaction Steps
Using methyl 4-propyl-1H-pyrrole-3-carboxylate (2.8 g), N-bromosuccinimide (3.0 g) and pyridine (0.5 mL), a procedure as in Reference Example 40 was performed to give the title compound as colorless crystals (yield 2.96 g, 72%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-20d437c3f94942dbbf3aea3bcffe48e9 |
| Source note | uspto-grants-2011_11 |