HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 15274277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 66924955 | HCID 66924955 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | HCID 15274277 | HCID 15274277 | 76% |
Reaction Steps
Using methyl 5-bromo-4-phenyl-1-(phenylsulfonyl)-1H-pyrrole-3-carboxylate (1.01 g), phenylboronic acid (439 mg), sodium carbonate (771 mg) and tetrakis(triphenylphosphine)palladium (420 mg), a procedure as in Reference Example 56 was performed to give the title compound as pale-yellow crystals (yield 506 mg, 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-81a5f5ad3e2e47a5a0a2f973630444a7 |
| Source note | uspto-grants-2011_11 |