HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorobenzenesulphonyl chloride → HCID 66924617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorobenzenesulphonyl chloride | HCID 17909 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 2-methyl-5-phenyl-1H-pyrrole-3-carboxylate | HCID 12258777 | — |
| Product | HCID 66924617 | HCID 66924617 | 49.3% |
Reaction Steps
Using ethyl 2-methyl-5-phenyl-1H-pyrrole-3-carboxylate (1.53 g), sodium hydride (60% in oil, 303 mg) and 3-chlorobenzenesulfonyl chloride (848 mg), a procedure as in Reference Example 41 was performed to give the title compound as a brown oil (yield 800 mg, 30%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-2eccb6185ae540b081c9b44777a9db78 |
| Source note | uspto-grants-2011_11 |