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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 554302Generated: October 28, 2026

Methyl morpholine oxide → HCID 86620745, compound

https://huagongshe.com/reaction/554302

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl morpholine oxideHCID 82029—
ReactantHCID 66924770HCID 66924770—
CatalystHCID 178419074HCID 178419074—
ProductHCID 86620745HCID 8662074570.1%

Reaction Steps

Using {1-[(3-chlorophenyl)sulfonyl]-2-methyl-5-phenyl-1H-pyrrol-3-yl}methanol (340 mg), tetra-n-propylammonium perruthenate (17.7 mg), N-methylmorpholine N-oxide (179 mg) and molecular sieves 4A powder (189 mg), a procedure as in Reference Example 6 was performed to give the title compound as a brown oil (yield 237 mg, 70%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08048909B2
Source datasetuspto-grants-2011_11
ORD IDord-154848a506c74c2eb14236d546a0373f
Source noteuspto-grants-2011_11