HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 66924994, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 66924874 | HCID 66924874 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | HCID 66924994 | HCID 66924994 | 37% |
Reaction Steps
Using tert-butyl {[5-bromo-4-isopropyl-1-(phenylsulfonyl)-1H-pyrrol-3-yl]methyl}methylcarbamate (596 mg), phenylboronic acid (307 mg), tetrakis(triphenylphosphine)palladium (218 mg) and sodium carbonate (401 mg), a procedure as in Reference Example 56 was performed to give the title compound as a pale-red oil (yield 218 mg, 37%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-1b4dc58d898b41acb36fef64233f8b99 |
| Source note | uspto-grants-2011_11 |