HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 66924971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Monomethylamine methanol | HCID 57454252 | — |
| Reactant | HCID 86620780 | HCID 86620780 | — |
| Product | HCID 66924971 | HCID 66924971 | 65% |
Reaction Steps
Using 1-[(1,1-dioxido-2,3-dihydro-1-benzothiophen-6-yl)sulfonyl]-5-phenyl-1H-pyrrole-3-carbaldehyde (114 mg), 40% methylamine methanol solution (0.3 mL) and sodium borohydride (10.8 mg), a procedure as in Example 126 was performed to give the title compound as a white solid (yield 76.3 mg, 65%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08048909B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-199d579bbbad4a719dda0f78ec47a3c6 |
| Source note | uspto-grants-2011_11 |