HCID 67460266, compound → HCID 11689581, compound

Participants

Reaction Steps

To a solution of 2-(4-ethylbenzyl)-1-methoxy-4-[(1S,2S,3R,4R,5R)-2,3,4-tris-benzyloxy-5-(benzyloxymethyl)cyclohexyl]benzene (10 mg, 0.013 mmol) in THF (0.2 mL) and methanol (1 mL), a 20% palladium hydroxide catalyst (10 mg) was added and the mixture was stirred under a hydrogen atmosphere at room temperature for 13 hours. After filtering the catalyst, the filtrate was concentrated under reduced pressure. The obtained residue was purified by preparative TLC [developing solution=methanol:methylene chloride (1:10)] to obtain the title compound (3.9 mg, 75%).

Provenance & Evidence