HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 55464Generated: October 28, 2026
Methanesulfonyl chloride → HCID 54255118, compound
https://huagongshe.com/reaction/55464
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 19078285 | HCID 19078285 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54255118 | HCID 54255118 | — |
Reaction Steps
3.8 ml of methanesulfonyl chloride are added dropwise to 21 g of 4-(2-hydroxyethyl)-4-(3-methyl-phenyl)-N-tritylpiperidine (prepared according to scheme 5) dissolved in 200 ml of methylene chloride, cooled to 0° C. The reaction mixture is left for half an hour at room temperature, washed twice with water, dried over MgSO4 and concentrated under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05625060 |
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| Source dataset | uspto-grants-1997_04 |
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| ORD ID | ord-728e6088b4664c1a972d6b26222916b1 |
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| Source note | uspto-grants-1997_04 |
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