Lactic Acid → HCID 86617049, compound

HRID 555190Notes

Reaction equation

HRID 555190 reaction equation
[C:1](O)(=[O:5])[CH:2]([CH3:4])[OH:3].[OH:7][CH:8]1[O:16][C@H:15]([CH2:17][OH:18])[C@@H:13]([OH:14])[C@H:11]([OH:12])[C@H:9]1[NH2:10]>>[C:1]([NH:10][C@@H:9]1[C@@H:11]([OH:12])[C@H:13]([OH:14])[C@@H:15]([CH2:17][OH:18])[O:16][CH:8]1[OH:7])(=[O:5])[CH:2]([CH3:4])[OH:3]

Participants

3

Reactant 2

HCID 612Lactic AcidHCID 439213D-Glucosamine

Product 1

HCID 86617049HCID 86617049, compound

Conditions

Temperature
120 °C

Procedure

Lactic acid (30 g) and glucosamine (10 g) were mixed and heated for 4 hours at 120° C. The reaction mixture was cooled and washed with ethyl acetate. The residue (25 g) was dissolved in 100 g of water.

Workup

  1. temperatureThe reaction mixture was cooled
  2. washwashed with ethyl acetate
  3. dissolutionThe residue (25 g) was dissolved in 100 g of water

Sources & evidence

ORD record
ord-2806e782ddeb4497973d4fb143885b27
Source dataset
uspto-grants-2011_11
Patent number
US08053013B2

Reaction notes

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