Ethanolamine → HCID 178523447, compound

HRID 555327Notes

Reaction equation

HRID 555327 reaction equation
CO[C:3]([C:5]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[N:8]=[C:7]([OH:15])[CH:6]=1)=[O:4].[CH2:16]([CH2:18][NH2:19])[OH:17]>C(Cl)(Cl)Cl>[OH:17][CH2:16][CH2:18][NH:19][C:3]([C:5]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[N:8]=[C:7]([OH:15])[CH:6]=1)=[O:4]

Participants

4

Reactant 2

HCID 700EthanolamineHCID 178498588HCID 178498588, compound

Product 1

HCID 178523447HCID 178523447, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

A solution of 4-methoxycarbonyl-2-hydroxyquinoline (40 mg) and ethanolamine (0.1 ml) in chloroform (5 ml) was stirred at 60° C. for 48 hours. After cooling the colourless product was isolated by filtration.

Workup

  1. temperatureAfter cooling the colourless product
  2. customwas isolated by filtration

Sources & evidence

ORD record
ord-023bdee94930485792804975ecf27887
Source dataset
uspto-grants-2011_11
Patent number
US08053446B2

Reaction notes

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