HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Tert-Butylaniline → HCID 59857420, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Tert-Butylaniline | HCID 69861 | — |
| Reactant | HCID 59857388 | HCID 59857388 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 59857420 | HCID 59857420 | 54.3% |
Reaction Steps
To a solution of 4-tert-butyl aniline (30 mg, 0.20 mmol) in DCE (2 mL) was slowly added 1c (50 mg, 0.17 mmol). The reaction was stirred 48 h at rt and concentrated. 96a was crystallized from methanol to afford 40 mg (52% yield) of white crystals. [M+H]+=434.04.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053450B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-fb0c511345d64491a3874010588c04c4 |
| Source note | uspto-grants-2011_11 |