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HRID555479

反应详情

EQUATION

反应方程式

HRID 555479 的结构方程式

REACTANTS

反应物

3
结构：NC(=O)c1ccccc1N
HCID6942

2-Aminobenzamide

C7H8N2O

结构：O=Cc1ccc(Oc2ncccn2)cc1
HCID2763562

4-(Pyrimidin-2-yloxy)benzaldehyde

C11H8N2O2

结构：COc1cc(OC)c2c(=O)[nH]c(-c3ccccn3)nc2c1
HCID136037998

未命名化合物

PRODUCTS

生成物

1
结构：O=c1[nH]c(-c2ccc3c(c2)OCCO3)nc2ccccc12
HCID136038020

未命名化合物

收率 72%

PROCEDURE

实验过程

2-(2,3-Dihydrobenzo[b][1,4]dioxin-6-yl)quinazolin-4(3H)-one was synthesized from anthranilamide and 4-(pyrimidin-2-yloxy)-benzaldehyde, using the method described for 5,7-dimethoxy-2-(pyridin-2-yl)quinazolin-4(3H)-one. 2-(2,3-Dihydrobenzo[b][1,4]dioxin-6-yl)quinazolin-4(3H)-one (222 mg, 72%) was isolated as a light beige solid. Selected data: MS (m/z): 280.98; MP 267-268° C. (decomposed).