HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dihydroxybenzohydrazide → N'-[1-[1-(3,4-dimethylphenyl)-3-methyl-5-oxopyrazol-4-ylidene]ethyl]-3,5-dihydroxybenzohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dihydroxybenzohydrazide | HCID 586309 | — |
| Reactant | HCID 178466978 | HCID 178466978 | — |
| Product | N'-[1-[1-(3,4-dimethylphenyl)-3-methyl-5-oxopyrazol-4-ylidene]ethyl]-3,5-dihydroxybenzohydrazide | HCID 178433871 | — |
Reaction Steps
From 1-(1-(3,4-dimethylphenyl)-5-hydroxy-3-methyl-1H-pyrazol-4-yl)-ethanone and 3,5-dihydroxybenzoic hydrazide, 57.0 mg of the desired product was obtained in the same manner as in Synthetic Example 1 as a pale red solid (yield 73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053453B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-03e42bb6f5af4064a24aac549bc75d53 |
| Source note | uspto-grants-2011_11 |