alpha-Hydrazino-m-cresol dihydrochloride → HCID 178422853, compound
Reaction equation
[C:1]1([N:7]2[C:11](=[O:12])[CH:10]([C:13](=O)[CH2:14][C:15](=O)[CH3:16])[C:9]([CH3:19])=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.Cl.[OH:22][C:23]1[CH:24]=[C:25]([CH:29]=[CH:30][CH:31]=1)[CH2:26][NH:27][NH2:28]>>[OH:22][C:23]1[CH:24]=[C:25]([CH:29]=[CH:30][CH:31]=1)[CH2:26][N:27]1[C:13]([C:10]2[C:9]([CH3:19])=[N:8][N:7]([C:1]3[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=3)[C:11]=2[OH:12])=[CH:14][C:15]([CH3:16])=[N:28]1Participants
3
Procedure
Prepare the title compound from 1-[1-phenyl-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl]-butane-1,3-dione and 3-hydroxybenzyl hydrazine dihydrochloride according to the procedure of Example 28.
Sources & evidence
- ORD record
- ord-114e6def0d9c469d9a4668b8de10a869
- Source dataset
- uspto-grants-2011_11
- Patent number
- US08053458B2
Reaction notes
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