Hydrazine, (phenylmethyl)-, hydrochloride (1:1) → HCID 178422852, compound
Reaction equation
[C:1]1([N:7]2[C:11](=[O:12])[CH:10]([C:13](=O)[CH2:14][C:15](=O)[CH3:16])[C:9]([CH3:19])=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH2:21]([NH:28][NH2:29])[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[CH2:21]([N:28]1[C:13]([C:10]2[C:9]([CH3:19])=[N:8][N:7]([C:1]3[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=3)[C:11]=2[OH:12])=[CH:14][C:15]([CH3:16])=[N:29]1)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1Participants
3
Procedure
Prepare the compound from 1-[1-phenyl-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl]-butane-1,3-dione and benzylhydrazine hydrochloride according to the procedure of Example 28.
Sources & evidence
- ORD record
- ord-8675dc572b6745cc9e6050250f0167e8
- Source dataset
- uspto-grants-2011_11
- Patent number
- US08053458B2
Reaction notes
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