Methylhydrazine → HCID 178422857, compound
Reaction equation
[C:1]1([N:7]2[C:11](=[O:12])[CH:10]([C:13](=O)[CH2:14][C:15](=O)[CH3:16])[C:9]([CH3:19])=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:20][NH:21][NH2:22]>>[CH3:20][N:21]1[C:13]([C:10]2[C:9]([CH3:19])=[N:8][N:7]([C:1]3[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=3)[C:11]=2[OH:12])=[CH:14][C:15]([CH3:16])=[N:22]1Participants
3
Procedure
Prepare the title compound from 1-[1-phenyl-3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-4-yl]-butane-1,3-dione and methylhydrazine according to the procedure of Example 28.
Sources & evidence
- ORD record
- ord-5637bb11adef4b6894ee03488dbbccef
- Source dataset
- uspto-grants-2011_11
- Patent number
- US08053458B2
Reaction notes
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