(Phenylmethyl)hydrazine → HCID 46193608, compound

HRID 555646Notes

Reaction equation

HRID 555646 reaction equation
[CH3:1][C:2]1[Se:6][C:5]([C:7]([C:9]2[O:10][C:11]([C:14]([O:16][CH3:17])=[O:15])=[CH:12][CH:13]=2)=O)=[CH:4][CH:3]=1.[CH2:18]([NH:25][NH2:26])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1.C(N1C2C=C[Se]C=2C(C2OC(C(OC)=O)=CC=2)=N1)C1C=CC=CC=1>C(O)(=O)C>[CH2:18]([N:25]1[C:4]2[CH:3]=[C:2]([CH3:1])[Se:6][C:5]=2[C:7]([C:9]2[O:10][C:11]([C:14]([O:16][CH3:17])=[O:15])=[CH:12][CH:13]=2)=[N:26]1)[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

5

Reactant 3

HCID 11157(Phenylmethyl)hydrazineHCID 46193253HCID 46193253, compoundHCID 46193500HCID 46193500, compound

Product 1

HCID 46193608HCID 46193608, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Compound 7 (5.94 g, 0.02 mole), benzylhydrazine 50 (4.88 g, 0.04 mole) and glacial acetic acid (1.5 ml) were allowed to react as in the preparation of compound 55 to afford compound 56. Yield: 1.56 g (19.5%); white crystals;

Sources & evidence

ORD record
ord-11b1f4324cd94cfb96e46dbd5d75ade4
Source dataset
uspto-grants-2011_11
Patent number
US08053459B1

Reaction notes

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