HCID 46193251, compound → HCID 46193610, compound

HRID 555652Notes

Reaction equation

HRID 555652 reaction equation
[C:1]1([N:7]2[C:11]3[CH:12]=[CH:13][Se:14][C:10]=3[C:9]([C:15]3[CH:20]=[CH:19][C:18]([C:21](OC)=[O:22])=[CH:17][CH:16]=3)=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(N1C2C=C[Se]C=2C(C2OC(C(OC)=O)=CC=2)=N1)C1C=CC=CC=1.C(N1C2C=C[Se]C=2C(C2OC(CO)=CC=2)=N1)C1C=CC=CC=1>>[C:1]1([N:7]2[C:11]3[CH:12]=[CH:13][Se:14][C:10]=3[C:9]([C:15]3[CH:16]=[CH:17][C:18]([CH2:21][OH:22])=[CH:19][CH:20]=3)=[N:8]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 3

HCID 46193251HCID 46193251, compoundHCID 46193500HCID 46193500, compoundHCID 461935011-Phenyl-3-(p-methoxycarbonylphenyl)selenolo[3,2-c]pyrazole

Product 1

HCID 46193610HCID 46193610, compound

Procedure

Compound 66 (0.764 g, 0.002 mole) was used to replace compound 55 in the preparation of compound 57 to afford compound 68. Yield: 0.585 g (82.9%); white needle crystals; mp 133-134° C.

Sources & evidence

ORD record
ord-23d326d8ef02467ebe90187f6aca837b
Source dataset
uspto-grants-2011_11
Patent number
US08053459B1

Reaction notes

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