HCID 46193251, compound → HCID 46193611, compound

HRID 555653Notes

Reaction equation

HRID 555653 reaction equation
[CH2:1]([N:8]1[C:12]2[CH:13]=[CH:14][Se:15][C:11]=2[C:10]([C:16]2[CH:21]=[CH:20][C:19]([C:22](OC)=[O:23])=[CH:18][CH:17]=2)=[N:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(N1C2C=C[Se]C=2C(C2OC(C(OC)=O)=CC=2)=N1)C1C=CC=CC=1.C(N1C2C=C[Se]C=2C(C2OC(CO)=CC=2)=N1)C1C=CC=CC=1>>[CH2:1]([N:8]1[C:12]2[CH:13]=[CH:14][Se:15][C:11]=2[C:10]([C:16]2[CH:17]=[CH:18][C:19]([CH2:22][OH:23])=[CH:20][CH:21]=2)=[N:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 46193251HCID 46193251, compoundHCID 46193500HCID 46193500, compoundHCID 46193502HCID 46193502, compound

Product 1

HCID 46193611HCID 46193611, compound

Procedure

Compound 67 (0.792 g, 0.002 mole) was used to replace compound 55 in the preparation of compound 57 to afford compound 69. Yield: 0.564 g (76.8%); white needle crystals; mp 158-160° C.

Sources & evidence

ORD record
ord-1092fe9ae5f44ae9977b94abb374cf6b
Source dataset
uspto-grants-2011_11
Patent number
US08053459B1

Reaction notes

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