HCID 46193500, compound → HCID 46193717, compound

HRID 555654Notes

Reaction equation

HRID 555654 reaction equation
[CH2:1]([N:8]1[C:12]2[CH:13]=[CH:14][Se:15][C:11]=2[C:10]([C:16]2[CH:21]=[CH:20][C:19]([C:22]([O:24]C)=[O:23])=[CH:18][CH:17]=2)=[N:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(N1C2C=C[Se]C=2C(C2OC(C(OC)=O)=CC=2)=N1)C1C=CC=CC=1.C(N1C2C=C[Se]C=2C(C2OC(C(O)=O)=CC=2)=N1)C1C=CC=CC=1>>[CH2:1]([N:8]1[C:12]2[CH:13]=[CH:14][Se:15][C:11]=2[C:10]([C:16]2[CH:21]=[CH:20][C:19]([C:22]([OH:24])=[O:23])=[CH:18][CH:17]=2)=[N:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 46193500HCID 46193500, compoundHCID 46193502HCID 46193502, compoundHCID 46193615HCID 46193615, compound

Product 1

HCID 46193717HCID 46193717, compound

Procedure

Compound 67 (0.792 g, 0.002 mole) was used to replace compound 55 in the preparation of compound 59 to afford compound 70. Yield: 0.649 g (85.2%); white crystals; mp 288-290° C.

Sources & evidence

ORD record
ord-97c546f9a844412786031bb8d709e3b8
Source dataset
uspto-grants-2011_11
Patent number
US08053459B1

Reaction notes

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