(Phenylmethyl)hydrazine → HCID 54588369, compound

HRID 555656Notes

Reaction equation

HRID 555656 reaction equation
COC(C1OC(C2[Se]C=CC=2[C:15]([C:17]2[CH:21]=[CH:20][Se:19][C:18]=2[C:22]2[O:23][C:24]([C:27]([O:29][CH3:30])=[O:28])=[CH:25][CH:26]=2)=O)=CC=1)=O.[CH2:31]([NH:38][NH2:39])[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1.C(N1C2C=C[Se]C=2C(C2OC(C(OC)=O)=CC=2)=N1)C1C=CC=CC=1>C(O)(=O)C>[CH2:31]([N:38]1[C:15]2[Se:19][CH:20]=[CH:21][C:17]=2[C:18]([C:22]2[O:23][C:24]([C:27]([O:29][CH3:30])=[O:28])=[CH:25][CH:26]=2)=[N:39]1)[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1

Participants

5

Reactant 3

HCID 11157(Phenylmethyl)hydrazineHCID 46193500HCID 46193500, compoundHCID 86761434HCID 86761434, compound

Product 1

HCID 54588369HCID 54588369, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Compound 73 (5.6 g, 0.02 mole), benzylhydrazine 50 (4.88 g, 0.04 mole) and glacial acetic acid (1.5 ml) were allowed to react as in the preparation of compound 55 to afford compound 79. Yield: 0.82 g (10.6%); white crystals;

Sources & evidence

ORD record
ord-d87841f4b2b54583a8388f0758ed8136
Source dataset
uspto-grants-2011_11
Patent number
US08053459B1

Reaction notes

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