HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetonitrile → (4-Ethylpiperazin-1-yl)acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetonitrile | HCID 11534 | — |
| Reactant | 1-Ethylpiperazine | HCID 79196 | — |
| Product | (4-Ethylpiperazin-1-yl)acetonitrile | HCID 22688890 | — |
Reaction Steps
The title compound is synthesized by coupling of 1-Ethyl-piperazine and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a orange oil; ES-MS: M+=154.1: 1HNMR(DMSO-d6) 3.70 (s, 2H), 2.40-2.20 (m, 10H), 0.95 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053457B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-afeccc5d3e064fe89e881a26b52a4572 |
| Source note | uspto-grants-2011_11 |