Bromoacetonitrile → HCID 60705436, compound

HRID 555737Notes

Reaction equation

[CH3:1][O:2][CH2:3][CH2:4][N:5]1[CH2:10][CH2:9][NH:8][CH2:7][CH2:6]1.Br[CH2:12][C:13]#[N:14]>>[CH3:1][O:2][CH2:3][CH2:4][N:5]1[CH2:10][CH2:9][N:8]([CH2:12][C:13]#[N:14])[CH2:7][CH2:6]1

Participants

Reactant 2

HCID 11534Bromoacetonitrile

HCID 27346381-(2-Methoxyethyl)piperazine

Product 1

HCID 60705436HCID 60705436, compound

Procedure

The title compound is synthesized by coupling of 1-(2-Methoxy-ethyl)-piperazine and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=184.2.

Sources & evidence

ORD record: ord-b75989a31d1746f38de064ddc397de45
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08053457B2

Reaction notes

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