Bromoacetonitrile → HCID 60964410, compound

HRID 555747Notes

Reaction equation

HRID 555747 reaction equation
[N:1]1([CH:7]2[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Br[CH2:14][C:15]#[N:16]>>[N:1]1([CH:7]2[CH2:12][CH2:11][N:10]([CH2:14][C:15]#[N:16])[CH2:9][CH2:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 11534BromoacetonitrileHCID 786071,4'-Bipiperidine

Product 1

HCID 60964410HCID 60964410, compound

Procedure

The title compound is synthesized by coupling of [1,4′]Bipiperidinyl (commercially available from Fluorochem Ltd) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+=208.2.

Workup

  1. customanalogously to the preparation of Intermediate 149.2 as a colorless oil

Sources & evidence

ORD record
ord-bdea8170b87344cbb60ff1c4c12ea0da
Source dataset
uspto-grants-2011_11
Patent number
US08053457B2

Reaction notes

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