huagongshe.com
HRID555779

反应详情

EQUATION

反应方程式

HRID 555779 的结构方程式

REACTANTS

反应物

2
结构：O=C(CN1CCNCC1)N1CCCC1
HCID100614

1-((Pyrrolidine-1-carbonyl)methyl)piperazine

C10H19N3O

结构：CC(C)(C)OC(=O)NCCBr
HCID4103526

tert-Butyl N-(2-bromoethyl)carbamate

C7H14BrNO2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCN1CCN(CC(=O)N2CCCC2)CC1
HCID66987566

未命名化合物

PROCEDURE

实验过程

The title compound is synthesized by coupling of 2-piperazin-1-yl-1-pyrrolidin-1-yl-ethanone (commercially available from CHESS GmbH) and (2-Bromo-ethyl)-carbamic acid tert-butyl ester analogously to the preparation of Intermediate 269.2 as a colorless oil; ES-MS: M+H=341.3: CtRet=4.08.

WORKUP

后处理

  1. customanalogously to the preparation of Intermediate 269.2 as a colorless oil