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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 555912Generated: November 1, 2026

4-Chlorobenzoyl chloride → HCID 178522174, compound

https://huagongshe.com/reaction/555912

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Chlorobenzoyl chlorideHCID 8501—
ReactantHCID 178507674HCID 178507674—
ProductHCID 178522174HCID 17852217437%

Reaction Steps

The title compound was prepared essentially according to the method of Example 4, but using 5-Chloro-2-(1H-tetrazol-5-yl)aniline (1.0 mmol) and 4-chlorobenzoyl chloride to yield the desired product (126.3 mg, 37%). 1H NMR (400 MHz, d6-DMSO): δ 13.62 (s, 1H), 8.87 (s, 1H), 8.22 (m, 3H), 7.72 (s, 2H), 7.25 (s, 1H). MS (EI) for C14H9Cl2N5O: 334.165 (M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08053454B2
Source datasetuspto-grants-2011_11
ORD IDord-66b9130650b04b51b3496158ef4995a8
Source noteuspto-grants-2011_11