HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-Enal → HCID 66987718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-Enal | HCID 307 | — |
| Reactant | HCID 9794806 | HCID 9794806 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 66987718 | HCID 66987718 | 95.2% |
Reaction Steps
20 mg Huperzine A, and 77 mg cinnamaldehyde were refluxed in 2 mL isopropanol for 3 hours. Solvent was removed under vacuum. The crude reaction mixture was dissolved in 3 mL anhydrous THF and purified with prep. TLC (CHCl3: methanol=9:1) to give 28 mg of title product. MS: 357 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08053577B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-daabc654b2c64a11a4837e1db0950023 |
| Source note | uspto-grants-2011_11 |