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HRID556261

反应详情

EQUATION

反应方程式

HRID 556261 的结构方程式

REACTANTS

反应物

1
结构：c1ccc(CN(Cc2ccccc2)[C@H]2CC[C@H](N3CCOCC3)CC2)cc1
HCID178420353

未命名化合物

PRODUCTS

生成物

1
结构：N[C@H]1CC[C@H](N2CCOCC2)CC1
HCID178511580

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

7.2 g (16.4 mmol) of trans-dibenzyl-4-morpholino-cyclohexylamine are dissolved in 100 mL of MeOH and hydrogenated on 1.4 g of Pd/C (10%) at 30-50° C. The solvent is eliminated in vacuo and the residue is crystallised from ethanol and concentrated HCl.

WORKUP

后处理

  1. customthe residue is crystallised from ethanol and concentrated HCl