HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Fluoro-4-formyl-phenyl)-acrylic acid tert-butyl ester → HCID 86235056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Fluoro-4-formyl-phenyl)-acrylic acid tert-butyl ester | HCID 86235053 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 86235056 | HCID 86235056 | 104.3% |
Reaction Steps
3-(3-fluoro-4-formyl-phenyl)-acrylic acid tert-butyl ester (2 g, 8 mmol) was dissolved in DCM (23 ml) and trifluoroacetic acid (6 ml). The mixture was stirred at room temperature for 6 h then the solvent was evaporated under vacuo giving 1.62 g of 3-(3-fluoro-4-formyl-phenyl)-acrylic acid
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058273B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-a716e369dd024fcaaa13c0e71e551b02 |
| Source note | uspto-grants-2011_11 |